Hydrazine → 3-Hydrazinyl-4-methyl-6-phenylpyridazine
Reaktionsgleichung
Cl[C:2]1[N:3]=[N:4][C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:6][C:7]=1[CH3:8].[NH2:15][NH2:16]>>[CH3:8][C:7]1[CH:6]=[C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:4]=[N:3][C:2]=1[NH:15][NH2:16]Komponenten
3
Reaktionsbedingungen
- Temperatur
- 100 °C
Versuchsvorschrift
3-Chloro-4-methyl-6-phenylpyridazine (0.510 g, 2.49 mmol) was dissolved in hydrazine (1.56 ml, 49.8 mmol) then the reaction mixture was heated at 100° C. for 1.5 hours. The precipitate that had formed in the mixture was collected and washed with iPrOH. The solid was dried under high vacuum to afford 1-(4-methyl-6-phenylpyridazin-3-yl)hydrazine as a pale yellow solid.
Aufarbeitung
- customThe precipitate that had formed in the mixture
- customwas collected
- washwashed with iPrOH
- customThe solid was dried under high vacuum
Quellen und Nachweise
- ORD-Eintrag
- ord-0aaa04e4545440fbb21e6d7d09654bb4
- Quelldatensatz
- uspto-grants-2013_09
- Patentnummer
- US08524900B2
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