HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Isopropanol → Urethane acrylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Isopropanol | HCID 3776 | — |
| Edukt | Aminopropyltrimethoxysilane | HCID 83756 | — |
| Edukt | 2-Ethyl-2-(hydroxymethyl)propane-1,3-diol;prop-2-enoic acid | HCID 25019176 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | Urethane acrylate | HCID 21863578 | — |
Reaktionsschritte
A mixture of 5.40 g of 3-aminopropyltrimethoxysilane, 6.80 g of hexanedioldiacrylate, 19.0 g of trimethylolpropane triacrylate, and 57.9 g of isopropanol is stirred at room temperature for 72 hours. To the mixture, 1.15 g of acetic acid is added, and the mixture is stirred for 5 minutes. Next, 56.2 g of NALCO 1034A is added under vigorous agitation. The resulting mixture is stirred at room temperature for 1 hour. 0.34 g of a solution of EBECRYL 1360 (50% by weight in PM glycol ether) and 1.80 g of DAROCUR 1173 are added. The resulting coating composition is stirred for an additional 30 minutes to ensure mixing.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08748506B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-7272e9fa9a1d4cdc835d147fbaf606e4 |
| Quellennotiz | uspto-grants-2014_06 |