Hydrogen Bromide → HCID 49758827, Verbindung

HRID 40557

Reaktionsgleichung

Reaktionsgleichung von HRID 40557
C[O:2][C:3]1[CH:8]=[CH:7][C:6]([C@@H:9]([NH2:11])[CH3:10])=[CH:5][CH:4]=1.[BrH:12]>>[BrH:12].[NH2:11][C@H:9]([C:6]1[CH:7]=[CH:8][C:3]([OH:2])=[CH:4][CH:5]=1)[CH3:10]

Komponenten

3

Edukt 2

HCID 260Hydrogen BromideHCID 793467(S)-1-(4-Methoxyphenyl)ethylamine

Produkt 1

HCID 49758827HCID 49758827, Verbindung

Reaktionsbedingungen

Temperatur
100 °C

Versuchsvorschrift

To 11.0 g (72.7 mmol) (S)-1-(4-methoxy-phenyl)-ethylamine is added carefully 30 mL HBr (30% in HOAc). The mixture is stirred at 100° C. for 4 h. After cooling down to r.t., the solvent is removed in vacuo and the residue is dried in vacuo. The resulting product is used without further purification.

Aufarbeitung

  1. temperatureAfter cooling down to r.t.
  2. customthe solvent is removed in vacuo
  3. customthe residue is dried in vacuo
  4. customThe resulting product is used without further purification

Quellen und Nachweise

ORD-Eintrag
ord-388579f90eae45a381a7f25c01287e36
Quelldatensatz
uspto-grants-2013_09
Patentnummer
US08530460B2

Verknüpfte Notizen

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