HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methylamine → n-Methyl-3-nitropyridin-4-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methylamine | HCID 6329 | — |
| Edukt | 4-Methoxy-3-nitropyridine | HCID 355832 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | n-Methyl-3-nitropyridin-4-amine | HCID 556016 | — |
Reaktionsschritte
2.36 g 4-methoxy-3-nitro-pyridine and 2.33 ml methylamine (40% in water) are refluxed in 25 ml of ethanol for 3 h. Then the reaction mixture is evaporated to dryness. 2.3 g product are obtained as a solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08754073B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-35e601a38c5e47dfb5ec3c8613cdef1f |
| Quellennotiz | uspto-grants-2014_06 |