1-Piperonylpiperazine → 4-Benzo[1,3]dioxol-5-ylmethyl-piperazine-1-carboxylic acid pyridin-3-ylamide

HRID 40595

Reaktionsgleichung

Reaktionsgleichung von HRID 40595
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][N:11]3[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]3)=[CH:9][C:4]=2[O:3][CH2:2]1.C([O:21][C:22]([N:24]1CC[N:27]([CH2:30][C:31]2[CH:39]=CC3OCOC=3C=2)[CH2:26][CH2:25]1)=O)(C)(C)C>>[N:27]1[CH:30]=[CH:31][CH:39]=[C:25]([NH:24][C:22]([N:14]2[CH2:13][CH2:12][N:11]([CH2:10][C:8]3[CH:7]=[CH:6][C:5]4[O:1][CH2:2][O:3][C:4]=4[CH:9]=3)[CH2:16][CH2:15]2)=[O:21])[CH:26]=1

Komponenten

3

Edukt 2

HCID 944261-PiperonylpiperazineHCID 687066184-Benzo[1,3]dioxol-5-ylmethyl-piperazine-1-carboxylic acid tert-butyl ester

Produkt 1

HCID 245286484-Benzo[1,3]dioxol-5-ylmethyl-piperazine-1-carboxylic acid pyridin-3-ylamide

Versuchsvorschrift

1-Benzo[1,3]dioxol-5-ylmethyl-piperazine. The title compound was prepared from 4-benzo[1,3]dioxol-5-ylmethyl-piperazine-1-carboxylic acid tert-butyl ester in analogy with Example 6.

Quellen und Nachweise

ORD-Eintrag
ord-f5f2eba130f1400d8ef6a7ecd6b16c11
Quelldatensatz
uspto-grants-2013_09
Patentnummer
US08530476B2

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