1-Piperonylpiperazine → 4-Benzo[1,3]dioxol-5-ylmethyl-piperazine-1-carboxylic acid pyridin-4-ylamide

HRID 40597

Reaktionsgleichung

Reaktionsgleichung von HRID 40597
C1(O[C:8](=[O:16])[NH:9][C:10]2[CH:15]=[CH:14][N:13]=[CH:12][CH:11]=2)C=CC=CC=1.[O:17]1[C:21]2[CH:22]=[CH:23][C:24]([CH2:26][N:27]3[CH2:32][CH2:31][NH:30][CH2:29][CH2:28]3)=[CH:25][C:20]=2[O:19][CH2:18]1>>[N:13]1[CH:12]=[CH:11][C:10]([NH:9][C:8]([N:30]2[CH2:31][CH2:32][N:27]([CH2:26][C:24]3[CH:23]=[CH:22][C:21]4[O:17][CH2:18][O:19][C:20]=4[CH:25]=3)[CH2:28][CH2:29]2)=[O:16])=[CH:15][CH:14]=1

Komponenten

3

Edukt 2

HCID 944261-PiperonylpiperazineHCID 11401617Carbamic acid, 4-pyridinyl-, phenyl ester

Produkt 1

HCID 578808584-Benzo[1,3]dioxol-5-ylmethyl-piperazine-1-carboxylic acid pyridin-4-ylamide

Versuchsvorschrift

The title compound was prepared from pyridin-4-yl-carbamic acid phenyl ester and 1-benzo[1,3]dioxol-5-ylmethyl-piperazine. 1H NMR (400 MHz, CDCl3): 8.33 (d, J=5.3 Hz, 2H), 7.35-7.34 (m, 2H), 6.79 (s, 1H), 6.68-6.67 (m, 2H), 5.89 (s, 2H), 3.48-3.45 (m, 4H), 3.39 (s, 2H), 2.43-2.40 (m, 4H).

Quellen und Nachweise

ORD-Eintrag
ord-8e9287760ba047bb8bf05d3433fb3a0a
Quelldatensatz
uspto-grants-2013_09
Patentnummer
US08530476B2

Verknüpfte Notizen

Wird geladen…