HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(3-Benzyloxy-phenoxy)-tert-butyl-dimethyl-silane → 3-(Tert-butyldimethylsilyl)oxy-1-cyclohexanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (3-Benzyloxy-phenoxy)-tert-butyl-dimethyl-silane | HCID 58421755 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-(Tert-butyldimethylsilyl)oxy-1-cyclohexanol | HCID 557077 | — |
Reaktionsschritte
A mixture of 37.6 g (3-benzyloxy-phenoxy)-tert-butyl-dimethyl-silane and 3.8 g of Nishimura's catalyst in 200 ml of ethanol was hydrogenated at rt under 50 psi for 6 hours. The reaction mixture was filtered and the filtrate concentrated.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08754079B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-733f331f4f134e8484831a22c5f587cc |
| Quellennotiz | uspto-grants-2014_06 |