4-Methoxyphenol → 4-Methoxycyclohexanol (cis,trans)

HRID 406050

Reaktionsgleichung

Reaktionsgleichung von HRID 406050
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([OH:9])=[CH:5][CH:4]=1.[H][H]>C(O)C>[CH3:1][O:2][CH:3]1[CH2:8][CH2:7][CH:6]([OH:9])[CH2:5][CH2:4]1

Komponenten

4

Edukt 2

HCID 90154-MethoxyphenolHCID 178418361HCID 178418361, Verbindung

Produkt 1

HCID 1403324-Methoxycyclohexanol (cis,trans)

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

A mixture of 100 g 4-methoxyphenol and Nishimura's catalyst in 750 ml ethanol were hydrogenated (50 psi hydrogen) at room temperature for 4.5 hours. The mixture was filtered and the filtrate was concentrated.

Aufarbeitung

  1. customat room temperature
  2. customfor 4.5 hours
  3. filtrationThe mixture was filtered
  4. concentrationthe filtrate was concentrated

Quellen und Nachweise

ORD-Eintrag
ord-eb53658046a44dc08b8875ac0fe90b71
Quelldatensatz
uspto-grants-2014_06
Patentnummer
US08754079B2

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