Urea → 6-iodo-1H-quinazoline-2,4-dione

https://huagongshe.com/de/reaction/40767

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Urea	HCID 1176	—
Edukt	Benzoic acid, 2-amino-5-iodo-	HCID 72911	—
Produkt	6-iodo-1H-quinazoline-2,4-dione	HCID 11380668	—

Reaktionsschritte

Prepared according to general method B from 2-amino-5-iodobenzoic acid (5.0 g) and urea (11.4 g). Yield: 5.34 g (98%) of a solid. 1H-NMR (DMSO-δ6) δ (ppm) 8.04 (d, J=2.0 Hz, 1H), 7.77 (dd, J=2.1 Hz, J=8.6 Hz, 1H), 6.90 (d, J=8.6 Hz, 1H).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08530486B2
Quelldatensatz	uspto-grants-2013_09
ORD ID	ord-9335f5568c75453ca70f906beb945760
Quellennotiz	uspto-grants-2013_09