HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methylamine → Methyl 4-(methylamino)-3-nitrobenzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methylamine | HCID 6329 | — |
| Edukt | Methyl 4-chloro-3-nitrobenzoate | HCID 735797 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Methyl 4-(methylamino)-3-nitrobenzoate | HCID 7650848 | — |
Reaktionsschritte
4-Methylamino-3-nitro-benzoic acid methyl ester (822 mg) was prepared by following General Procedure A starting from methyl 4-chloro-3-nitrobenzoate (1.0 g) and methylamine (2 M in THF, 6.95 mL) in DMF. The crude product was used in the next step without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08759535B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-7f3c860dc8984f65a22b71e866d028cd |
| Quellennotiz | uspto-grants-2014_06 |