HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 4-(methylamino)-3-nitrobenzoate → Methyl 3-amino-4-(methylamino)benzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 4-(methylamino)-3-nitrobenzoate | HCID 7650848 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Produkt | Methyl 3-amino-4-(methylamino)benzoate | HCID 15586064 | 96,1% |
Reaktionsschritte
3-amino-4-methylamino-benzoic acid methyl ester (677 mg) was prepared by following General Procedure B starting from 4-methylamino-3-nitro-benzoic acid methyl ester (822 mg) and Pd/C (10% by weight, 82 mg). The crude product was used in the next step without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08759535B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-4518beb51d0246db85a61f63cb1016c4 |
| Quellennotiz | uspto-grants-2014_06 |