HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Amino-6-methylbenzothiazole → HCID 58397627, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Amino-6-methylbenzothiazole | HCID 17335 | — |
| Edukt | 1,1'-Thiocarbonyldiimidazole | HCID 80264 | — |
| Edukt | Methyl 3-amino-4-(methylamino)benzoate | HCID 15586064 | — |
| Lösungsmittel | 1,2-Dichloroethane | HCID 11 | — |
| Produkt | HCID 58397627 | HCID 58397627 | 83,5% |
Reaktionsschritte
1-Methyl-2-(6-methyl-benzothiazol-2-ylamino)-1H-benzoimidazole-5-carboxylic acid methyl ester (1.47 g) was prepared by following General Procedure D starting from 3-amino-4-methylamino-benzoic acid methyl ester (0.9 g), 2-amino-6-methyl-benzothiazole (0.82 g), 1,1′-thiocarbonyldiimidazole (1.07 g), and EDC (1.15 g). LC/MS: m/z 354.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08759535B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-ea4992c285a04c8a86ae1c6ff5a5a075 |
| Quellennotiz | uspto-grants-2014_06 |