Sodium Azide → 1-Azido-2-(2-methoxyethoxy)ethane

HRID 410980

Reaktionsgleichung

Br[CH2:2][CH2:3][O:4][CH2:5][CH2:6][O:7][CH3:8].[N-:9]=[N+:10]=[N-:11].[Na+]>>[N:9]([CH2:2][CH2:3][O:4][CH2:5][CH2:6][O:7][CH3:8])=[N+:10]=[N-:11]

Komponenten

Edukt 2

HCID 33557Sodium Azide

HCID 1235321-Bromo-3,6-dioxaheptane

Produkt 1

HCID 100347511-Azido-2-(2-methoxyethoxy)ethaneAusbeute 76,5 %

Versuchsvorschrift

1-Azido-2-(2-methoxy-ethoxy)-ethane (607 mg) was prepared by following General Procedure U starting from 1-bromo-2-(2-methoxy-ethoxy)-ethane (1.0 g) and sodium azide (1.07 g). The crude product was used in the next step without further purification.

Aufarbeitung

customThe crude product was used in the next step without further purification

Quellen und Nachweise

ORD-Eintrag: ord-da46aa2df9f94867b4ddaed513066231
Quelldatensatz: uspto-grants-2014_06
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08759535B2

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