Thionyl Chloride → 4-(Methylamino)-3-nitrobenzoyl chloride

HRID 411049

Reaktionsgleichung

Reaktionsgleichung von HRID 411049
[CH3:1][NH:2][C:3]1[CH:11]=[CH:10][C:6]([C:7](O)=[O:8])=[CH:5][C:4]=1[N+:12]([O-:14])=[O:13].S(Cl)([Cl:17])=O>>[CH3:1][NH:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([Cl:17])=[O:8])=[CH:5][C:4]=1[N+:12]([O-:14])=[O:13]

Komponenten

3

Edukt 2

HCID 24386Thionyl ChlorideHCID 2834754-(Methylamino)-3-nitrobenzoic acid

Produkt 1

HCID 179464494-(Methylamino)-3-nitrobenzoyl chloride

Reaktionsbedingungen

Temperatur
80 °C

Versuchsvorschrift

4-Methylamino-3-nitro-benzoyl chloride (4.3 g) was prepared starting from 4-methylamino-3-nitro-benzoic acid (4 g) in thionyl chloride (20 mL). The reaction was heated to 80° C. for 8 h. The solvent was evaporated to isolate pure compound without any further purification.

Aufarbeitung

  1. customThe solvent was evaporated
  2. customto isolate pure compound
  3. customwithout any further purification

Quellen und Nachweise

ORD-Eintrag
ord-cf67af8299fd443997516bc33d342552
Quelldatensatz
uspto-grants-2014_06
Patentnummer
US08759535B2

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