Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 411428Erstellt: 25. Oktober 2026

tert-Butyl bromoacetate → N-(3,4-dichlorophenyl)alanine Tert-butyloxycarbonylmethyl Ester

https://huagongshe.com/reaction/411428

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukttert-Butyl bromoacetateHCID 79177—
EduktN-(3,4-dichlorophenyl)alanineHCID 5491659—
ProduktN-(3,4-dichlorophenyl)alanine Tert-butyloxycarbonylmethyl EsterHCID 54406316—

Reaktionsschritte

Following General Procedure AE above and using N-(3,4-dichlorophenyl)alanine (from Example AB above) and tert-butyl bromoacetate (Aldrich), the title compound was prepared as a solid. The reaction was monitored by silica gel tlc (Rf=0.57 in 25% EtOAc/hexanes). Purification was by recrystallization from ethanol.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06559141B2
Quelldatensatzuspto-grants-2003_05
ORD IDord-ec2cd4f582e846b8bdbace523e827e05
Quellennotizuspto-grants-2003_05