HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,4-Tetrahydrothiazine-3-one → 4-Benzylthiomorpholin-3-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,4-Tetrahydrothiazine-3-one | HCID 88402 | — |
| Edukt | 4-(Bromomethyl)-1,2-dichlorobenzene | HCID 639726 | — |
| Edukt | 4-(3,4-Dichlorobenzyl)-thiomorpholin-3-one | HCID 12083011 | — |
| Produkt | 4-Benzylthiomorpholin-3-one | HCID 14941172 | — |
Reaktionsschritte
In the same manner, 4-(3,4-dichlorobenzyl)-thiomorpholin-3-one was prepared in 89% yield from 3,4-dichlorobenzyl bromide and thiomorpholin-3-one as a white solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06562813B2 |
| Quelldatensatz | uspto-grants-2003_05 |
| ORD ID | ord-d12fb8c7dd2a482b9551ddcb7e9bccb7 |
| Quellennotiz | uspto-grants-2003_05 |