2-Ethoxybenzoyl chloride → 2-(2-Ethoxybenzamido)-3-methylbenzamide
Reaktionsgleichung
[NH2:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5].[CH2:12]([O:14][C:15]1[CH:23]=[CH:22][CH:21]=[CH:20][C:16]=1[C:17](Cl)=[O:18])[CH3:13]>>[CH2:12]([O:14][C:15]1[CH:23]=[CH:22][CH:21]=[CH:20][C:16]=1[C:17]([NH:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5])=[O:18])[CH3:13]Komponenten
3
Versuchsvorschrift
The title compound was prepared from 2-amino-3-methylbenzamide (Chem. Pharm. Bull., 1988, 36, 2955) and 2-ethoxybenzoyl chloride following the procedure of Preparation 5 and was obtained as colourless crystals (71%), m.p. 197-200° C.
Aufarbeitung
- customthe procedure of Preparation 5
Quellen und Nachweise
- ORD-Eintrag
- ord-ca8550a7f4c8409fb25406d710a9893b
- Quelldatensatz
- uspto-grants-2003_05