HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → Furan-2-acetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | 2-Furanacetonitrile | HCID 10909515 | — |
| Produkt | Furan-2-acetic acid | HCID 75974 | — |
Reaktionsschritte
A mixture of 2-furanacetonitrile (6.14 g), KOH (4.0 g), and water (25 mL) was refluxed for 1 hour and then cooled. Following extraction with ether, the aqueous layer was acidified to pH 2.0 with concentrated aqueous HCl. This solution was extracted with ether, and the organic phase was dried over MgSO4 and evaporated under vacuum to yield 2-furanacetic acid. The structure of the product was confirmed by NMR.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06566508B2 |
| Quelldatensatz | uspto-grants-2003_05 |
| ORD ID | ord-dc1b7ed696e7453f8c2cfc7d65c6a3d5 |
| Quellennotiz | uspto-grants-2003_05 |