Reaktionsgleichung
[CH3:1][CH:2]([CH2:6][CH2:7][CH2:8][CH3:9])[C:3](O)=[O:4].[NH2:10][C@H:11]([C:13]([N:15]1[C:21](=[O:22])[CH:20]([CH3:23])[C:19]2[CH:24]=[CH:25][CH:26]=[CH:27][C:18]=2[C:17]2[C:28]([NH2:32])=[CH:29][CH:30]=[CH:31][C:16]1=2)=[O:14])[CH3:12]>>[CH3:1][CH:2]([CH2:6][CH2:7][CH2:8][CH3:9])[C:3]([NH:10][C@H:11]([C:13]([N:15]1[C:21](=[O:22])[CH:20]([CH3:23])[C:19]2[CH:24]=[CH:25][CH:26]=[CH:27][C:18]=2[C:17]2[C:28]([NH2:32])=[CH:29][CH:30]=[CH:31][C:16]1=2)=[O:14])[CH3:12])=[O:4]Komponenten
3
Versuchsvorschrift
Following General Procedure C-P above using 2-methylhexanoic acid and 5-(L-alaninyl)-amino-7-methyl-5,7-dihydro-6H-dibenz[b,d]azepin-6-one, as described in Example 7-B, the title compound was prepared. The molecular weight as determined by mass spectrometry (FD) was: 422 (M+H).
Quellen und Nachweise
- ORD-Eintrag
- ord-ab365075308c402089e3b8d668d7d6b6
- Quelldatensatz
- uspto-grants-2003_05
- Patentnummer
- US06569851B1
Verknüpfte Notizen
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