HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanolamine → 2-(Aminomethyl)phenol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanolamine | HCID 700 | — |
| Edukt | Formaldehyde | HCID 712 | — |
| Edukt | Phosphoric Acid | HCID 1004 | — |
| Edukt | 4-tert-Butylphenol | HCID 7393 | — |
| Lösungsmittel | Water ethanol | HCID 19096565 | — |
| Produkt | 2-(Aminomethyl)phenol | HCID 70267 | — |
Reaktionsschritte
An o-hydroxybenzylamine compound of the present invention composition was prepared according to the procedure of Example 1, except that 50 g of 4-t-butylphenol was employed in place of the Bisphenol-A, 20.1 g of ethanolamine was employed in place of the 2-(methylamino)ethanol, and that heating of the reactants was only begun after the formaldehyde addition was completed. A 0.5 g sample of the product was dissolved in 500 ml of ethanol/water (1:4 by volume) and the pH of the solution was adjusted to 3.0 with phosphoric acid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04792355 |
| Quelldatensatz | uspto-grants-1988_12 |
| ORD ID | ord-7486f9fc336349f2b2dc1e0a870090b4 |
| Quellennotiz | uspto-grants-1988_12 |