Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Calcium Carbonate | HCID 10112 | — |
| Edukt | Sulfur | HCID 5362487 | — |
| Edukt | endo-Dicyclopentadiene | HCID 15618652 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | HCID 178419798 | HCID 178419798 | — |
Reaktionsschritte
Into a 4 liter autoclave were placed 425 g of sulfur, 75 g of DCPD, 2500 ml of water and 20 g of calcium carbonate. The reactor was then sealed and heated to 150° C. for three hours with stirring. After cooling to ambient temperature, the sulfur/DCPD adduct was isolated as small beads.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US04792589 |
|---|
| Quelldatensatz | uspto-grants-1988_12 |
|---|
| ORD ID | ord-0005c5c1607a4f3f973b1472511c893f |
|---|
| Quellennotiz | uspto-grants-1988_12 |
|---|
