HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sulfuric Acid → 4-Methyl-6-aminomethyl-7-hydroxy-1-indanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | 4-Methyl-6-alpha-chloroacetylaminomethyl-7-hydroxy-1-indanone | HCID 13604141 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 4-Methyl-6-aminomethyl-7-hydroxy-1-indanone | HCID 13604144 | — |
Reaktionsschritte
3 Grams of 4-methyl-6-α-chloroacetylaminomethyl-7-hydroxy-1-indanone and a solution of 30 ml of concentrated sulfuric acid in 60 ml of ethanol were refluxed by heating for 8 hours. The solvent was removed by evaporation, the residue thus obtained was recrystallized from ethanol to obtain 1 g of 4-methyl-6-aminomethyl-7-hydroxy-1-indanone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04792628 |
| Quelldatensatz | uspto-grants-1988_12 |
| ORD ID | ord-d178894b4e4c4482b7509e98b99d4b09 |
| Quellennotiz | uspto-grants-1988_12 |