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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 41498Erstellt: 23. Oktober 2026

Hydrochloric Acid → HCID 68817634, Verbindung

https://huagongshe.com/de/reaction/41498

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrochloric AcidHCID 313—
EduktDimethyl SulfoxideHCID 679—
Eduktmethyl N-[3-(6,7-dimethoxy-2-methylaminoquinazolin-4-yl)phenyl]terephthalamic acidHCID 66646296—
LösungsmittelIsopropanolHCID 3776—
ProduktHCID 68817634HCID 68817634—

Reaktionsschritte

Dimethyl sulfoxide (1 mL) and hydrochloric acid (22 μL) were added to methyl N-[3-(6,7-dimethoxy-2-methylaminoquinazolin-4-yl)phenyl]terephthalamic acid (99.37 mg). Dimethyl sulfoxide (2 mL) was added to and dissolved in the mixture while heating the mixture, 2-propanol (3 mL) was added to the mixture, and the mixture was cooled to room temperature to be solidified. The solid was collected by filtration to yield the titled compound (88.65 mg).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08530654B2
Quelldatensatzuspto-grants-2013_09
ORD IDord-d69699ced6d04373b7ba39101758b8fe
Quellennotizuspto-grants-2013_09