HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrogen Bromide → HCID 68820841, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrogen Bromide | HCID 260 | — |
| Edukt | Dimethyl Sulfoxide | HCID 679 | — |
| Edukt | methyl N-[3-(6,7-dimethoxy-2-methylaminoquinazolin-4-yl)phenyl]terephthalamic acid | HCID 66646296 | — |
| Lösungsmittel | Isopropanol | HCID 3776 | — |
| Produkt | HCID 68820841 | HCID 68820841 | — |
Reaktionsschritte
Dimethyl sulfoxide (1 mL) and hydrobromic acid (40 μL) were added to methyl N-[3-(6,7-dimethoxy-2-methylaminoquinazolin-4-yl)phenyl]terephthalamic acid (100.90 mg). 2-Propanol (5 mL) was added to the mixture while heating the mixture, and the mixture was cooled to room temperature to be solidified. The solid was collected by filtration to yield the titled compound (108.92 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08530654B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-c3aa049b7aa9465693f6054ed6d6261f |
| Quellennotiz | uspto-grants-2013_09 |