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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 41499Erstellt: 23. Oktober 2026

Hydrogen Bromide → HCID 68820841, Verbindung

https://huagongshe.com/de/reaction/41499

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrogen BromideHCID 260—
EduktDimethyl SulfoxideHCID 679—
Eduktmethyl N-[3-(6,7-dimethoxy-2-methylaminoquinazolin-4-yl)phenyl]terephthalamic acidHCID 66646296—
LösungsmittelIsopropanolHCID 3776—
ProduktHCID 68820841HCID 68820841—

Reaktionsschritte

Dimethyl sulfoxide (1 mL) and hydrobromic acid (40 μL) were added to methyl N-[3-(6,7-dimethoxy-2-methylaminoquinazolin-4-yl)phenyl]terephthalamic acid (100.90 mg). 2-Propanol (5 mL) was added to the mixture while heating the mixture, and the mixture was cooled to room temperature to be solidified. The solid was collected by filtration to yield the titled compound (108.92 mg).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08530654B2
Quelldatensatzuspto-grants-2013_09
ORD IDord-c3aa049b7aa9465693f6054ed6d6261f
Quellennotizuspto-grants-2013_09