Hydrochloric Acid → 1,3,5-Tris-(p-(dec-1-yloxycarbonyl)-anilino)-s-triazine

HRID 4158

Reaktionsgleichung

Reaktionsgleichung von HRID 4158
[NH2:1][C:2]1[CH:20]=[CH:19][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[O:7])=[CH:4][CH:3]=1.[N:21]1[C:28](Cl)=[N:27][C:25](Cl)=[N:24][C:22]=1Cl.Cl>C1(C)C(C)=CC=CC=1>[CH2:9]([O:8][C:6]([C:5]1[CH:4]=[CH:3][C:2]([NH:1][N:21]2[CH2:28][N:27]([NH:1][C:2]3[CH:20]=[CH:19][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[O:7])=[CH:4][CH:3]=3)[CH2:25][N:24]([NH:1][C:2]3[CH:3]=[CH:4][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[O:7])=[CH:19][CH:20]=3)[CH2:22]2)=[CH:20][CH:19]=1)=[O:7])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 7954Cyanuric chlorideHCID 4446056Decyl 4-aminobenzoate

Produkt 1

HCID 201527341,3,5-Tris-(p-(dec-1-yloxycarbonyl)-anilino)-s-triazine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 7237O-XyleneLösungsmittel

Reaktionsbedingungen

Temperatur
90 °C

Versuchsvorschrift

83 g of decyl p-aminobenzoate and 18.5 g of cyanuric chloride in 1,000 ml of xylene were heated at 140° C. for 8 hours. After the evolution of hydrogen chloride was complete, the reaction solution was cooled to 90° C., washed twice with saturated sodium bicarbonate solution and once with water, and then cooled to room temperature. The white crystals precipitated were filtered off under suction and dried.

Aufarbeitung

  1. washwashed twice with saturated sodium bicarbonate solution and once with water
  2. temperaturecooled to room temperature
  3. customThe white crystals precipitated
  4. filtrationwere filtered off under suction
  5. customdried

Quellen und Nachweise

ORD-Eintrag
ord-d7ec7c5243894addb439002cd6f1f99a
Quelldatensatz
uspto-grants-1988_02
Patentnummer
US04724137

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