HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diethyl Sulfate → N-ethyl phenazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diethyl Sulfate | HCID 6163 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | Ethoxyethane;phenazine | HCID 67351390 | — |
| Produkt | N-ethyl phenazine | HCID 15309770 | — |
Reaktionsschritte
Scheme 6 illustrates the synthesis of N-ethyl phenazine 1-hydroxybutyl methyl ether. The phenazine ether (21) is prepared by the alkylation of the 1-hydroxyphenazine (1) with 4-methoxybutylbromide (Aldrich Chemical Company, USA) to give phenazine derivative (21). N-ethyl phenazine (22) is prepared by reaction of compound (21) with diethyl sulfate in the presence of potassium carbonate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08535511B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-b95dea2c26064186aaec0a2320d0234f |
| Quellennotiz | uspto-grants-2013_09 |