4-Bromo-1-methyl-1H-imidazole → HCID 59424524, Verbindung

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	4-Bromo-1-methyl-1H-imidazole	HCID 1277653	—
Edukt	7-chloro-2-(1-methyl-1H-imidazol-2-yl)-thieno[3,2-b]pyridine	HCID 22143563	—
Produkt	HCID 59424524	HCID 59424524	—

Reaktionsschritte

Following the procedure described for compound 7 (example 2, step 3) but substituting 2-bromo-1-methyl-1H-imidazole for 4-bromo-1-methyl-1H-imidazole [a) Begtrup, M.; Larsen, P.; Acta Chem. Scand. 44, 10; 1990; 1050-1057. b) Begtrup, M.; Bull. Soc. Chim. Belg.; 97; 8-9; 1988; 573-598. c) Begtrup, M.; Larsen, P.; Chem. Pharm. Bull. 42, 9; 1994; 1784-1790.], title compound 10 was obtained as an off-white solid (29% yield). MS (m/z): 250.1 (M+H).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08093264B2
Quelldatensatz	uspto-grants-2012_01
ORD ID	ord-467b536abbd246dea821eb8675d2d03b
Quellennotiz	uspto-grants-2012_01