4-Chloro-N-methoxy-N-methylbenzamide → HCID 57942543, Verbindung

HRID 419002

Reaktionsgleichung

Reaktionsgleichung von HRID 419002
Br[C:2]1[C:7]([N:8](COC)[S:9]([C:12]2[CH:17]=[CH:16][C:15]([Cl:18])=[C:14]([C:19]([F:22])([F:21])[F:20])[CH:13]=2)(=[O:11])=[O:10])=[CH:6][C:5]([Cl:26])=[CH:4][N:3]=1.[Cl:27][C:28]1[CH:39]=[CH:38][C:31]([C:32](N(OC)C)=[O:33])=[CH:30][CH:29]=1>>[Cl:18][C:15]1[CH:16]=[CH:17][C:12]([S:9]([NH:8][C:7]2[C:2]([C:32](=[O:33])[C:31]3[CH:38]=[CH:39][C:28]([Cl:27])=[CH:29][CH:30]=3)=[N:3][CH:4]=[C:5]([Cl:26])[CH:6]=2)(=[O:10])=[O:11])=[CH:13][C:14]=1[C:19]([F:21])([F:22])[F:20]

Komponenten

3

Edukt 2

HCID 112756634-Chloro-N-methoxy-N-methylbenzamideHCID 57942086N-(2-Bromo-5-chloro-pyridin-3-yl)-4-chloro-N-methoxvmethyl-3-trifluoromethyl-benzenesulfonamide

Produkt 1

HCID 57942543HCID 57942543, Verbindung

Versuchsvorschrift

The title compound was prepared by procedure analogous to that described in Example 29 using N-(2-bromo-5-chloro-pyridin-3-yl)-4-chloro-N-methoxymethyl-3-trifluoromethyl-benzenesulfonamide and 4-chloro-N-methoxy-N-methyl-benzamide 1H NMR (400 MHz, CDCl3) δ10.61 (s, 1H), 8.37 (m, 1H), 8.16 (m, 1H), 8.09 (m, 1H), 7.84 (m, 1H), 7.77-7.75 (m, 2H), 7.53 (m, 1H), 7.42-7.40 (m, 2H), 7.23 (m, 1H) MS: (M+H)/z=509.0.

Quellen und Nachweise

ORD-Eintrag
ord-39de2979ca3f4967b38db498465588bd
Quelldatensatz
uspto-grants-2012_01
Patentnummer
US08093247B2

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