HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(Trifluoromethoxy)phenylboronic Acid (contains varying amounts of Anhydride) → 3-Methyl-5-nitro-2-(3-(trifluoromethoxy)phenyl)pyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(Trifluoromethoxy)phenylboronic Acid (contains varying amounts of Anhydride) | HCID 2734385 | — |
| Edukt | 2-Bromo-3-methyl-5-nitropyridine | HCID 5200466 | — |
| Produkt | 3-Methyl-5-nitro-2-(3-(trifluoromethoxy)phenyl)pyridine | HCID 67393780 | 91% |
Reaktionsschritte
Obtained (1.25 g, yield 91%) following the procedure described in Intermediate 27, starting with 2-bromo-3-methyl-5-nitropyridine (4.61 mmol, 1.0 g), 3-(trifluoromethoxy)phenyl boronic acid (4.61 mmol, 0.95 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08536165B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-7da434c3faf646b18a54584636098cab |
| Quellennotiz | uspto-grants-2013_09 |