HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(3-Carbamoylphenyl)boronic acid → 3-(3-Methyl-5-nitropyridin-2-yl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (3-Carbamoylphenyl)boronic acid | HCID 2737814 | — |
| Edukt | 2-Bromo-3-methyl-5-nitropyridine | HCID 5200466 | — |
| Produkt | 3-(3-Methyl-5-nitropyridin-2-yl)benzamide | HCID 67394166 | 95% |
Reaktionsschritte
Obtained (0.225 g, yield 95%) following the procedure described in Intermediate 27, starting with 2-bromo-3-methyl-5-nitropyridine (0.92 mmol, 0.200 g), 3-carbamoylphenyl boronic acid (0.92 mmol, 0.152 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08536165B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-7f080017fac3419a8fc81fdf3499b97c |
| Quellennotiz | uspto-grants-2013_09 |