HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N,N-Dimethyl-N-decylamine → N-(2-methoxyethyl)-N,N-dimethyldecan-1-aminium bromide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N,N-Dimethyl-N-decylamine | HCID 70711 | — |
| Edukt | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | N-(2-methoxyethyl)-N,N-dimethyldecan-1-aminium bromide | HCID 71399801 | — |
Reaktionsschritte
The reaction was performed in an inert atmosphere. N,N-dimethyldecylamine (16.21 mmol, 3.7 g) and 2-bromoethyl methyl ether (16.21 mmol, 2.25 g) were mixed together in a round bottom flask. Acetone (10 mL) was added to the reaction mixture. The reaction mixture was heated to reflux for 8 hours. The solvent was removed by a rotoevaporator and remaining viscous liquid was cooled and dried. A brownish white solid was obtained as N-(2-methoxyethyl)-N,N-dimethyldecan-1-aminium bromide. By using this method other surfactants were also synthesized. Other surfactants were also synthesized by heating in dioxane at 75° C. for 10 hours instead of using acetone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08101556B2 |
| Quelldatensatz | uspto-grants-2012_01 |
| ORD ID | ord-7c10d6a3342b44d4b1fee377fec938d3 |
| Quellennotiz | uspto-grants-2012_01 |