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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 421545Erstellt: 25. Oktober 2026

N,N-Dimethyl-N-decylamine → N-(2-methoxyethyl)-N,N-dimethyldecan-1-aminium bromide

https://huagongshe.com/reaction/421545

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktN,N-Dimethyl-N-decylamineHCID 70711—
Edukt2-Bromoethyl methyl etherHCID 80972—
LösungsmittelAcetoneHCID 180—
ProduktN-(2-methoxyethyl)-N,N-dimethyldecan-1-aminium bromideHCID 71399801—

Reaktionsschritte

The reaction was performed in an inert atmosphere. N,N-dimethyldecylamine (16.21 mmol, 3.7 g) and 2-bromoethyl methyl ether (16.21 mmol, 2.25 g) were mixed together in a round bottom flask. Acetone (10 mL) was added to the reaction mixture. The reaction mixture was heated to reflux for 8 hours. The solvent was removed by a rotoevaporator and remaining viscous liquid was cooled and dried. A brownish white solid was obtained as N-(2-methoxyethyl)-N,N-dimethyldecan-1-aminium bromide. By using this method other surfactants were also synthesized. Other surfactants were also synthesized by heating in dioxane at 75° C. for 10 hours instead of using acetone.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08101556B2
Quelldatensatzuspto-grants-2012_01
ORD IDord-7c10d6a3342b44d4b1fee377fec938d3
Quellennotizuspto-grants-2012_01