2-Chloro-4-(methylsulfonyl)benzoic acid → Nicotinamide

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	2-Chloro-4-(methylsulfonyl)benzoic acid	HCID 735863	—
Edukt	N-(5-Amino-2-chlorophenyl)nicotinamide	HCID 28867202	—
Produkt	Nicotinamide	HCID 936	—

Reaktionsschritte

N-(5-amino-2-chlorophenyl)nicotinamide (0.40 mmol) was used in general procedure 2 with 2-chloro-4-(methylsulfonyl)benzoic acid (0.48 mmol). The product was purified by RP-HPLC to give N-(2-chloro-4-(methylsulfonyl)benzamido)phenyl)nicotinamide. MS (Q1) 464.0 (M)+

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08101610B2
Quelldatensatz	uspto-grants-2012_01
ORD ID	ord-1e1bd51e940d40f0a15ca1091c84de62
Quellennotiz	uspto-grants-2012_01