Dimethylamine → Sodium 2-(dimethylamino)ethanesulfonate

HRID 424670

Reaktionsgleichung

Reaktionsgleichung von HRID 424670
[CH2:1]=[CH:2][S:3]([O-:6])(=[O:5])=[O:4].[Na+:7].[CH3:8][NH:9][CH3:10]>>[CH3:8][N:9]([CH3:10])[CH2:1][CH2:2][S:3]([O-:6])(=[O:5])=[O:4].[Na+:7]

Komponenten

3

Edukt 2

HCID 674DimethylamineHCID 3270262Sodium vinylsulfonate

Produkt 1

HCID 23516383Sodium 2-(dimethylamino)ethanesulfonate

Versuchsvorschrift

Sodium ethylenesulfonate (18.2 ml, 25% aqueous solution w/w) and dimethylamine (4.43 ml, 40% aqueous solution w/w) were heated in a sealed finger tube at 105° C. for 48 h before concentrating in vacuo to yield the subtitle compound as a white solid. Yield: 9.80 g.

Aufarbeitung

  1. concentrationbefore concentrating in vacuo

Quellen und Nachweise

ORD-Eintrag
ord-3b9b1bfe3c984dff9ebaf9513b9644c9
Quelldatensatz
uspto-grants-2012_01
Patentnummer
US08106063B2

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