HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cannabidiol → Tetrahydrocannabinol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cannabidiol | HCID 644019 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | Tetrahydrocannabinol | HCID 16078 | — |
Reaktionsschritte
To a solution of cannabidiol (500 mg) in dichloromethane (8.75 mL) at 20° C., was added a solution of an organoaluminum-based Lewis acid catalyst in dichloromethane (1.0 mL) over five minutes and the reaction mixtures stirred under nitrogen and monitored by HPLC. Table 1 below shows the relative HPLC quantitation of the different product compounds in area percent at the time specified, using different organoaluminum-based Lewis acid catalysts.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08106244B2 |
| Quelldatensatz | uspto-grants-2012_01 |
| ORD ID | ord-2f7608101a864ea995147c28e9941511 |
| Quellennotiz | uspto-grants-2012_01 |