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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 42690Erstellt: 23. Oktober 2026

(2-Bromophenyl)boronic acid → 5-(2-Bromophenyl)-1,3-benzodioxole-4-carbaldehyde

https://huagongshe.com/de/reaction/42690

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt(2-Bromophenyl)boronic acidHCID 2773294—
Edukt5-Bromo-1,3-benzodioxole-4-carboxaldehydeHCID 11031640—
Produkt5-(2-Bromophenyl)-1,3-benzodioxole-4-carbaldehydeHCID 86658680—

Reaktionsschritte

The process described in Method B was followed. 5-Bromo-1,3-benzodioxole-4-carbaldehyde (1.15 g, 5.00 mmol) and 2-bromophenylboronic acid (1.10 g, 5.50 mmol) were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of hexane:ethyl acetate (9:1) as the eluent.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08536210B2
Quelldatensatzuspto-grants-2013_09
ORD IDord-89304411dabb487c91269d35b72d6f0f
Quellennotizuspto-grants-2013_09