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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 42692Erstellt: 24. Oktober 2026

Methanol → HCID 58484330, Verbindung

https://huagongshe.com/de/reaction/42692

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethanolHCID 887—
Edukt6-Chloro-5-formyl-1,3-dimethyluracilHCID 319971—
ProduktHCID 58484330HCID 58484330—

Reaktionsschritte

The process described in Method C was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.270 g, 1.33 mmol) and methanol were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of n-hexane:ethyl acetate (4:1) as the eluent.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08536210B2
Quelldatensatzuspto-grants-2013_09
ORD IDord-c85dff6070af47f89ad63f95a7464379
Quellennotizuspto-grants-2013_09