Methanol → HCID 58484330, Verbindung

HRID 42692

Reaktionsgleichung

Reaktionsgleichung von HRID 42692
Cl[C:2]1[N:7]([CH3:8])[C:6](=[O:9])[N:5]([CH3:10])[C:4](=[O:11])[C:3]=1[CH:12]=[O:13].[CH3:14][OH:15]>>[CH3:14][O:15][C:2]1[N:7]([CH3:8])[C:6](=[O:9])[N:5]([CH3:10])[C:4](=[O:11])[C:3]=1[CH:12]=[O:13]

Komponenten

3

Edukt 2

HCID 887MethanolHCID 3199716-Chloro-5-formyl-1,3-dimethyluracil

Produkt 1

HCID 58484330HCID 58484330, Verbindung

Versuchsvorschrift

The process described in Method C was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.270 g, 1.33 mmol) and methanol were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of n-hexane:ethyl acetate (4:1) as the eluent.

Quellen und Nachweise

ORD-Eintrag
ord-c85dff6070af47f89ad63f95a7464379
Quelldatensatz
uspto-grants-2013_09
Patentnummer
US08536210B2

Verknüpfte Notizen

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