HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzene → 4-Vinylpyridine styrene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzene | HCID 241 | — |
| Edukt | Azobisisobutyronitrile | HCID 6547 | — |
| Edukt | Styrene | HCID 7501 | — |
| Edukt | 2-Vinylpyridine | HCID 7521 | — |
| Lösungsmittel | Hexane | HCID 8058 | — |
| Produkt | 4-Vinylpyridine styrene | HCID 12666455 | 20% |
Reaktionsschritte
In a 200 ml three necked flask were charged 21 g of 4-vinylpyridine, 21 g of styrene and 0.1 g of azobisisobutyronitrile and 90 ml of benzene. The mixture was polymerized at 80° C. for 6 hrs under a nitrogen atmosphere. The reaction liquid was poured into a large amount of n-hexane to thereby obtain white precipitates. After filtering and drying, a white powder was obtained. The molar fraction of vinylpyridine in the polymer was 0.57 and the yield was 20%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04172180 |
| Quelldatensatz | uspto-grants-1979_10 |
| ORD ID | ord-31e2e703769040e5a59f3f08d630c2bc |
| Quellennotiz | uspto-grants-1979_10 |