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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 42697Erstellt: 25. Oktober 2026

Ethanethiol → 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

https://huagongshe.com/reaction/42697

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthanethiolHCID 6343—
Edukt6-Chloro-5-formyl-1,3-dimethyluracilHCID 319971—
Produkt6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehydeHCID 58484335—

Reaktionsschritte

The process described in Method D was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.303 g, 1.50 mmol) and ethanethiol were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of n-hexane:ethyl acetate (1:1) as the eluent.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08536210B2
Quelldatensatzuspto-grants-2013_09
ORD IDord-dbafb17038e6410e997a1aa39eb95162
Quellennotizuspto-grants-2013_09