HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanethiol → 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanethiol | HCID 6343 | — |
| Edukt | 6-Chloro-5-formyl-1,3-dimethyluracil | HCID 319971 | — |
| Produkt | 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde | HCID 58484335 | — |
Reaktionsschritte
The process described in Method D was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.303 g, 1.50 mmol) and ethanethiol were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of n-hexane:ethyl acetate (1:1) as the eluent.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08536210B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-dbafb17038e6410e997a1aa39eb95162 |
| Quellennotiz | uspto-grants-2013_09 |