3-(Methylthio)phenylacetic acid → N-[(3-methylthiophenyl)acetyl]alanine Iso-butyl Ester

HRID 428101Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 428101
[CH3:1][S:2][C:3]1[CH:4]=[C:5]([CH2:9][C:10]([OH:12])=O)[CH:6]=[CH:7][CH:8]=1.[CH2:13]([O:17][C:18](=[O:29])[C@H:19]([CH3:28])[NH:20]C(=O)CC(C)CC)[CH:14]([CH3:16])[CH3:15]>>[CH2:13]([O:17][C:18](=[O:29])[C@H:19]([CH3:28])[NH:20][C:10](=[O:12])[CH2:9][C:5]1[CH:6]=[CH:7][CH:8]=[C:3]([S:2][CH3:1])[CH:4]=1)[CH:14]([CH3:16])[CH3:15]

Komponenten

3

Edukt 2

HCID 27374613-(Methylthio)phenylacetic acidHCID 15481764N-(3-methylpentanoyl)-L-alanine Isobutyl Ester

Produkt 1

HCID 15481777N-[(3-methylthiophenyl)acetyl]alanine Iso-butyl Ester

Versuchsvorschrift

Following General Procedure I above, and using 3-methylthiophenylacetic acid (CAS# 18698-73-2) and alanine iso-butyl ester (prepared following General Procedure 3 above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.

Aufarbeitung

  1. customThe reaction was monitored by tlc on silica gel and purification
  2. filtrationwas by filtration

Quellen und Nachweise

ORD-Eintrag
ord-aad9369707694701a2c1aa38ab0ea626
Quelldatensatz
uspto-grants-2001_11
Patentnummer
US06313152B1

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