HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-Bromoindole → 5-Bromo-3-(1,4-dioxaspiro[4.5]dec-7-en-8-yl)-1H-indole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-Bromoindole | HCID 24905 | — |
| Edukt | 3-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-1H-indole | HCID 2763857 | — |
| Produkt | 5-Bromo-3-(1,4-dioxaspiro[4.5]dec-7-en-8-yl)-1H-indole | HCID 2763989 | 78% |
Reaktionsschritte
This compound was prepared in the manner described above for intermediate 1a by replacing indole with 5-bromoindole (7.84 g, 40 mmol) ) to afford 10.5 g (78%) of the title compound as a white solid; MS EI m/e 333 (M+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06313126B1 |
| Quelldatensatz | uspto-grants-2001_11 |
| ORD ID | ord-3ee30fe089e346e7b74c0d501545e657 |
| Quellennotiz | uspto-grants-2001_11 |