2,4,5-Trimethoxybenzaldehyde → 3-Hydroxy-3-(2,4,5-trimethoxyphenyl)-1-propyne

Beteiligte Stoffe

Reaktionsschritte

3-Hydroxy-3-(2,4,5-trimethoxyphenyl)-1-propyne was prepared according to Method A above from 2,4,5-trimethoxybenzaldehyde (0.784 g, 4 mmol) (Aldrich) in THF (20 mL) and ethynylmagnesium chloride (5 mmol, 10 mL, 0.5M solution in tetrahydrofuran) (Aldrich). (Yield 548 mg, 71%).

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