HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Nitrophthalic acid → 3-nitro-N-hydroxyphthalimide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Nitrophthalic acid | HCID 69043 | — |
| Edukt | Hydroxylammonium phosphate (3:1) | HCID 10176537 | — |
| Produkt | 3-nitro-N-hydroxyphthalimide | HCID 4659220 | — |
Reaktionsschritte
Analogous to Example 4, but from 500 mg (2.37 mmol) of 3-nitrophthalic acid and 187 mg (0.947 mmol) of hydroxylammonium phosphate at a bath temperature of 130° C. The yield was 443 mg (90%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06316639B1 |
| Quelldatensatz | uspto-grants-2001_11 |
| ORD ID | ord-b5b27bf38b6943a2b32bc2ef19e358e4 |
| Quellennotiz | uspto-grants-2001_11 |