HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethyl Sulfide → Trimethylsulfonium Triflate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethyl Sulfide | HCID 1068 | — |
| Edukt | Methyl triflate | HCID 9526 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | Trimethylsulfonium Triflate | HCID 10933171 | — |
Reaktionsschritte
16 mmol of dimethyl sulfide was dissolved in 10 ml of dichloromethane at 0° C., and about 17 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture to obtain a white solid product. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08536347B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-5cc9413dfef7447db1b13d03a866a5a8 |
| Quellennotiz | uspto-grants-2013_09 |