HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-[2-(2,4-Dichlorophenyl)ethoxy]-4-methoxybenzoic acid ethyl ester → 3-[2-(2,4-Dichlorophenyl)ethoxy]-4-methoxybenzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-[2-(2,4-Dichlorophenyl)ethoxy]-4-methoxybenzoic acid ethyl ester | HCID 15480331 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Lösungsmittel | Sodium Hydroxide | HCID 14798 | — |
| Produkt | 3-[2-(2,4-Dichlorophenyl)ethoxy]-4-methoxybenzoic acid | HCID 15480332 | 73% |
Reaktionsschritte
A solution of 3.6 g (9.8 mmol) of 3-[2-(2,4-dichlorophenyl)ethoxy]4-methoxybenzoic acid ethyl ester in 30 ml of ethanol and 5.4 ml of 2N sodium hydroxide solution was stirred at room temperature for 12 h. The precipitate was filtered off. The resulting solid was stirred with 5 ml of 2N HCl and filtered to give 2.44 g (73%) of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06664393B2 |
| Quelldatensatz | uspto-grants-2003_12 |
| ORD ID | ord-34e3e639d5814b65982c9730a9c1df44 |
| Quellennotiz | uspto-grants-2003_12 |