HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
tert-Butyl bromoacetate → N-(3,4-dichlorophenyl)alanine Tert-butyloxycarbonylmethyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | tert-Butyl bromoacetate | HCID 79177 | — |
| Edukt | N-(3,4-dichlorophenyl)alanine | HCID 5491659 | — |
| Produkt | N-(3,4-dichlorophenyl)alanine Tert-butyloxycarbonylmethyl Ester | HCID 54406316 | — |
Reaktionsschritte
Following General Procedure AE above and using N-(3,4-dichlorophenyl)alanine (from Example AB above) and tert-butyl bromoacetate (Aldrich), the title compound was prepared as a solid. The reaction was monitored by silica gel tlc (Rf=0.57 in 25% EtOAc/hexanes). Purification was by recrystallization from ethanol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06667305B1 |
| Quelldatensatz | uspto-grants-2003_12 |
| ORD ID | ord-46b88333463f4c1eb863f4c4af99c8bb |
| Quellennotiz | uspto-grants-2003_12 |