Sodium Hydroxide → 1-(4-Acetylphenyl) propan-2-ol

Reaktionsgleichung

C([O:4][CH:5]([CH3:16])[CH2:6][C:7]1[CH:12]=[CH:11][C:10]([C:13](=[O:15])[CH3:14])=[CH:9][CH:8]=1)(=O)C.[OH-].[Na+]>>[C:13]([C:10]1[CH:11]=[CH:12][C:7]([CH2:6][CH:5]([OH:4])[CH3:16])=[CH:8][CH:9]=1)(=[O:15])[CH3:14]

Komponenten

Edukt 2

HCID 14798Sodium Hydroxide

HCID 204938272-Acetoxy-1-(4-acetylphenyl)propane

Produkt 1

HCID 225984461-(4-Acetylphenyl) propan-2-olAusbeute 104,4 %

Versuchsvorschrift

2-Acetoxy-1-(4-acetylphenyl) propane (4.5 g) was heated for 2 hours in refluxing 2 N sodium hydroxide solution. The mixture was allowed to cool and the product was extracted into ether. Evaporation of the dried (MgSO4) extracts gave an oil (3.8 g).

Aufarbeitung

temperatureto cool
extractionthe product was extracted into ether
customEvaporation of the
dry with materialdried (MgSO4)

Quellen und Nachweise

ORD-Eintrag: ord-f3d02f20e0444b7eb09a5c9a270b63d0
Quelldatensatz: uspto-grants-1983_08
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04396627

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