HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Aniline → N-phenylcarbamoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Aniline | HCID 6115 | — |
| Edukt | Phosgene | HCID 6371 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | N-phenylcarbamoyl chloride | HCID 576741 | — |
Reaktionsschritte
The intermediate is then reacted with a secondary amine in an aprotic solvent such as toluene at temperatures from room temperature or below up to the boiling point of the solvent. An example of this process is the reaction of phosgene with aniline to yield the intermediate N-(phenyl)carbamyl chloride which is then reacted with N-benzyl-n-butylamine to yield 1-benzyl-1-(n-butyl)-3-(phenyl)urea.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04397868 |
| Quelldatensatz | uspto-grants-1983_08 |
| ORD ID | ord-e87810831aea4dcca6a2fde26a49ebcc |
| Quellennotiz | uspto-grants-1983_08 |