N-bromobutanimide → HCID 68405898, Verbindung
Reaktionsgleichung
[CH3:1][C:2]1[NH:6][C:5]([C:7]([O:9][CH2:10][CH3:11])=[O:8])=[N:4][CH:3]=1.C1C(=O)N([Br:19])C(=O)C1>>[Br:19][C:3]1[N:4]=[C:5]([C:7]([O:9][CH2:10][CH3:11])=[O:8])[NH:6][C:2]=1[CH3:1]Komponenten
3
Versuchsvorschrift
The same operation as in Example (1c) was performed using ethyl 5-methyl-1H-imidazole-2-carboxylate obtained by the method described in Example (5a) (0.30 g, 1.95 mmol) and NBS (0.35 g, 1.96 mmol), to obtain 0.43 g of the title compound as a white solid (94%).
Aufarbeitung
- customobtained by the method
Quellen und Nachweise
- ORD-Eintrag
- ord-d693ef5b612a4617add9d3780e2fbc6a
- Quelldatensatz
- uspto-grants-2013_09
- Patentnummer
- US08536197B2
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