Sulfuric Acid → 4-Amino-3-nitrobenzophenone

HRID 435484

Reaktionsgleichung

Reaktionsgleichung von HRID 435484
C([NH:4][C:5]1[CH:18]=[CH:17][C:8]([C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:10])=[CH:7][C:6]=1[N+:19]([O-:21])=[O:20])(=O)C.S(=O)(=O)(O)O>>[NH2:4][C:5]1[CH:18]=[CH:17][C:8]([C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:10])=[CH:7][C:6]=1[N+:19]([O-:21])=[O:20]

Komponenten

3

Edukt 2

HCID 1118Sulfuric AcidHCID 5969694-Acetamido-3-nitrobenzophenone

Produkt 1

HCID 5969704-Amino-3-nitrobenzophenone

Versuchsvorschrift

Ten grams of 4-acetamido-3-nitrobenzophenone were added portionwise to 40 ml. of sulfuric acid. The reaction temperature was moderated with a water bath. After stirring about 45 minutes the reaction mixture was carefully poured over ice. The precipitated product was filtered to yield 4-amino-3-nitrobenzophenone.

Aufarbeitung

  1. customThe reaction temperature was moderated with a water bath
  2. additionwas carefully poured over ice
  3. filtrationThe precipitated product was filtered

Quellen und Nachweise

ORD-Eintrag
ord-4f2cc8e00d8145e98418d2bf2ce66346
Quelldatensatz
uspto-grants-1983_08
Patentnummer
US04401817

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